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Microsegregation of Ti and Mn in a nitrogen-poor Fe –Ti– Mn–C alloy has been investigated experimentally and explained by a theoretical model. The formation of TiN precipitates in the residual melt of a nitrogen containing alloy has been detected and described by the model of homogeneous nucleation. The microsegregation is very high at the end of the solidification process, but the segregation zones are strongly widened during cooling in the delta ferrite. Precipitation of Ti nitride takes place in regions of the melt where the concentration product [%Ti][%N] exceeds the solubility product  L  TiN  by more than a factor 10. The same supersaturation level is required by the theory of homogeneous nucleation.

Segregation and Precipitation during Solidification of Titanium and Nitrogen Containing Iron Alloys