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This work concerns the reaction acceleration in bubble enhanced devolatilization (DV) occurring in reactive extrusion (REX), to provide further evidence that overall reactivity can be enhanced by boiling. Using monoesterification of a styrenemaleic anhydride copolymer with an alcohol as a model reaction, the rate increase was determined by comparing the conversions of the samples collected at different screw locations with those predicted from the combined kinetic equation for the bubble free homogeneous system and the RTD information obtained from both the RTD measurements and theoretical calculations.

Acceleration of Chemical Reaction in Reactive Extrusion Accompained by Devolatilization