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In this work, the results of the examinations of morphology and chemical composition of the primary AlTMSi intermetallic phases precipitates observed in the Al–Si cast alloys microstructure have been presented. A procedure for the treatment of EDS X-ray microanalysis results (selection and classification) using fuzzy logic concept has been developed and then tested in application for AlTMSi phase identification. Statistically significant differences in the chemical composition have been revealed between the analyzed groups of precipitates of both α- and β-AlTMSi phases formed in hypo- and eutectic Al-Si alloys with the same content of transition metals. The range of the measured Mn solubility in the precipitates of different crystal lattices has been statistically estimated.

A Procedure for in situ Identification of the Intermetallic AlTMSi Phase Precipitates in the Microstructure of the Aluminum Alloys