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Ni 0.5 Cu 0.5 Fe 2 O 4  nanocrystalline spinel ferrite was synthesized through a lactose monohydrate (C 12 H 22 O 11  · H 2 O) mediated chemical preparation technique (post annealed at 600°C for 4 h). Various analytical results obtained after characterization measurements such as X-ray powder diffraction, ultra violet–visible spectroscopy and Fourier transform infrared spectroscopy measurements were discussed. X-ray diffraction pattern analysis confirmed the formation of nanocrystalline face-centered cubic lattice phase of Ni 0.5 Cu 0.5 Fe 2 O 4  with crystallite size  ∼ 9 nm. The Tauc plot corresponding to ultra violet–visible reflectance data employing the Kubelka– Munk function provided a direct transition band gap of 4.92 eV. The characteristic tetrahedral and octahedral vibration bands observed in the Fourier transform infrared spectrum further confirmed that Ni 0.5 Cu 0.5 Fe 2 O 4  nanoparticles were crystallized in spinel structure.

Lactose monohydrate (C 12 H 22 O 11 · H 2 O) mediated synthesis and spectral analysis of nanocrystalline Ni 0.5 Cu 0.5 Fe 2 O 4