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Mechanochemically synthesized metal–organic framework material HKUST-1 in combination with acrylonitrile butadiene styrene polymer was used to form a polymer metal–organic framework composite material by a simple extruder. This composite filament was used for 3D printing. X-ray diffraction measurements were used to prove the homogeneous distribution of the metal–organic framework in the polymer on a centimeter scale, whereas X-ray Absorption Edge Tomography using a synchrotron radiation source was able to evaluate the 3D distribution of the metal–organic framework material both in the filament and the resultant printed sample with a resolution of a few μm. Our very first data indicate that, apart from a few clusters having significantly higher Cu concentration, HKUST-1 is distributed homogeneously down to the 100 μm length scale in both polymer bulk materials in the form of clusters with a size of a few μm. Absorption Edge Tomography in combination with data fusion also allows for the calculation of the metal–organic framework amount located on the external polymer surface.

international journal of materials research

Microstructure of polymer-imprinted metal–organic frameworks determined by absorption edge tomography: Paper presented at the Symposium “Tomographic and Radiographic Imaging with Synchrotron X-rays and Neutrons” of the MSE 2018, 26–28 September 2018, Darmstadt, Germany