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The [Zr(OH) 5 ] −  imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO 2  by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO 2  nanostructures.

Formation of zirconia precursor nanoplates mediated by ionic liquid and transformation to monoclinic ZrO 2 nanostructures