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The substructures and crystallographic features of martensite in 1.01C high-carbon steel were investigated using transmission electron microscopy and electron backscatter diffraction scanning electron microscopy. The results indicated that the “new” thin-plate martensite (M2), formed at cryogenic temperatures, possessed unique substructures and crystallographic features, which were quite different from the “original” large lenticular martensite (M1) formed at relatively high temperatures. Furthermore, the M1 and M2 can be distinguished and quantified using the band-contrast distributions from backscatter diffraction scanning electron microscopy.

The substructures and crystallographic features of martensite in high-carbon steel after cryogenic treatment