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Three-dimensional (3D) nanocomposite monolith containing MoS 2  nanoflakes, graphene oxide (GO) and amorphous SiO 2  was fabricated through a simple mixing process and hydrothermal treatment. Compared with GO monolith prepared under identical conditions, the MoS 2 –GO monolith had larger specific surface area, smaller pore diameter, as well as much higher adsorption capacity for Cu 2+  and Rhodamine B. Introducing amorphous SiO 2  into the end monolith by using tetraethyl orthosilicate as a reactant in the synthesis reduced shrinkage and produced a greater number of large pores (&gt;1 μm pore diameter) in the monolith. The specific surface area and pore diameter of the MoS 2 –GO monolith were 321.4 m 2  g −1  and 11.71 nm, respectively. The higher adsorption capacity was ascribed to the presence of many S atoms in the MoS 2  nanoflakes inside the monolith.

Fabrication of 3D porous MoS 2 –GO nanocomposite monolith as a promising adsorbent