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In this article, a new method of synthesis of ultrafine powder solid solution (Ti,W)C by a combination of classical liquid-phase precipitation on a carbon support and low-temperature microwave heat treatment is proposed. An entire spectrum of intermediates obtained during thermolysis, reduction, and carbidization precursor to the final product has been obtained. The structure, particle morphology, phase structure and surface area values for the samples are shown.

Synthesis of ultrafine powder (W,Ti)C by microwave heating in a stream of argon