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High-strength Ti 66 Nb 13 Cu 8 Ni 6.8 Al 6.2  composites with intermetallic matrix reinforced by nanocrystalline WC particles were fabricated via spark plasma sintering and crystallization of amorphous phase. Microstructure analysis indicates that the bulk composites contain isolated nanocrystalline WC particles surrounded by crystallized intermetallic matrix, including ductile bcc β-Ti regions surrounded by a mixed-phase region of (Cu, Ni)-Ti 2 , TiC, and remaining amorphous phase. With increasing sintering temperature the crystallized intermetallic matrix transforms from nanocrystalline to an ultrafine-grained structure. The composite with ultrafine-grained intermetallic matrix reinforced by 4.5 vol.% WC exhibits high yield and fracture strengths of 2194 and 2277 MPa, respectively. The variation of fracture strength for the fabricated composites can be explained based on the volume fraction of the crystallized ductile β-Ti phase and the scale of the crystallized phase regions.

international journal of materials research

Microstructure and mechanical properties of nanocrystalline WC-particle-reinforced Ti-based composites with nano/ultrafine-grained intermetallic matrix from spark plasma sintering and crystallization of amorphous phase