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Mg-10Gd-3Y-1.8Zn-0.5Zr (wt.%) alloy is prepared by permanent mold casting and further by slow solidification at cooling rate of 0.1 K s −  1 . Both X phase with long period stacking ordered structure and DO 3 -type (Mg,Zn) 3  RE  phase in the alloy are observed with electron microscopy and X-ray diffraction. Three different X phase/(Mg,Zn) 3  RE  phases are observed in the alloy. The orientation relationship between X phase and (Mg,Zn) 3  RE  phase was determined by the composite diffraction patterns, which can be expressed as (0014) X phase //(110) (  Mg,Zn  )3RE  and [110] X phase //[ 3  32] (  Mg,Zn  )3RE , (0014) X phase //(110) (  Mg,Zn  )3RE  and [110] X phase //[ 1  11] (  Mg,Zn  )3RE , (0014) X phase //(110) (  Mg,Zn  )3RE  and [210] X phase //[ 1  12] (  Mg,Zn  )3RE . These results show coherence between X phase and (Mg,Zn) 3  RE  phase and a very small mismatch in the phase boundaries.

Orientation relationship between 14H-LPSO structured X phase and DO 3 -type (Mg,Zn) 3 RE phase in an Mg–Gd–Y–Zn–Zr alloy