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A bulk nanostructured Ni 50 Al 17 Fe 33  alloy was produced by combustion synthesis associated with rapid solidification. The microstructure and mechanical properties of the as-fabricated material were investigated by means of scanning electron microscopy, X-ray diffraction, and mechanical tests. The Ni 50 Al 17 Fe 33  alloy was composed of eutectic matrix and precipitated phase. The eutectic matrix consisted of 30–50 nm globular γ′-(Ni,Fe) 3 Al and 5–10 nm γ-Ni(Fe) boundary. The precipitate was comprised of 100–150 nm γ′-(Ni,Fe) 3 Al, γ-Fe, and α-Fe solid solution phases. The nanostructured Ni 50 Al 17 Fe 33  alloy exhibited simultaneously high yield stress (about 900 MPa), high fracture strength (over 3860 MPa), and good ductility (over 75%) in compression.

Combustion synthesis and characterization of bulk nanostructured Ni 50 Al 17 Fe 33 alloy