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An electroless, room temperature solution growth method of depositing 50 to 150 μm thick, well-crystallized brushite (CaHPO 4  · 2H 2 O, DCPD, dicalcium phosphate dihydrate) layers on the surface of an implantable medical device, such as a titanium alloy (Ti–6Al–4V) substrate, was developed. High ionic strength (189 to 609 mM) solutions with a Ca/P molar ratio of 2.50 and a pH value between 4.70 and 6.10 were prepared by dissolving appropriate quantities of CaCl 2  · 2H 2 O, NaH 2 PO 4 , NaHCO 3 , and NaCl in deionized water. Surface-etched Ti–6Al–4V substrates were simply soaked in the solutions from 24 to 72 hours at room temperature. Elongated CaHPO 4  · 2H 2 O crystals were in-situ- grown on the entire surfaces of the etched Ti–6Al–4V substrates.

Electroless deposition of brushite (CaHPO 4 · 2H 2 O) crystals on Ti–6Al–4V at room temperature