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The present paper outlines the use of the novel polydentate Schiff's base extractant, N,N′-bis(2-hydroxy-1-naphthalideneaminoethyl)amine (H 2 L), for copper(II) extraction in aqueous two-phase micellar of non-ionic surfactant from sulphate media. The extraction process is based on the formation of the hydrophobic complex of copper(II)-H 2 L, which is subsequently extracted into the non-ionic surfactant-rich phase of p-octylpolyethyleneglycolphenylether (Triton X-100) at a temperature above the cloud point temperature (CPT). The phase diagrams of the binary system, water-surfactant (Triton X-100), and of the ternary systems, water-surfactant-salt (Na 2 SO 4 ), were examined. The effects of the main experimental parameters such as pH, extractant concentration and non-ionic surfactant concentration on the extraction process of copper(II) were studied. The extraction yield was found to be significantly depending on the aqueous solution pH. Copper(II) was extracted with H 2 L and Triton X-100 in the pH range of (3–12). From the equilibrium slope analysis method, it was suggested that the stoichiometry of the extracted complexes have a composition of 1:1 (Cu:H 2 L). The optimum conditions of the extraction of copper(II) have been established as the following: (1) 2 × 10 −3  M extractant; (2) 5% (m/v) surfactant; (3) pH of 7.2; (4) 7% (m/v) Na 2 SO 4  and (5) temperature of 65°C.

tenside surfactants detergents

Extraction of Copper(II) from Sulphate Aqueous Medium with N,N′-bis(2-hydroxy-1-naphthalideneaminoethyl)amine Polydentate Schiff Base in Aqueous Two-phase Micellar of Non-Ionic Surfactant