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Metalworking fluids (MWF)  are used routinely throughout the world as cooling and lubricating agent for metal-cutting processes. They are important components to maintain the quality and precision of the metal-cutting but are slowly consumed within this process. Hence, monitoring of ageing of the MWFs before depletion is important for economical, ecological and security reasons. A method is presented, which enables to estimate the ageing of tools by measuring the microbial volatile outcome (MVOC) of the MWF. Measurements are done by headspace sorptive extraction combined to thermal desorption in a gas chromatography setup with mass selective detector (HSSE-TDS-GCMS). It could be shown that ageing of tools correlates to emission of ketonic and alcoholic MVOCs (namely 2-Heptanone, 2-Octanone, 1-Octanol, 2-Nonanone and 2-Decanone). Analysis of these components can be used as “ageing marker” for the investigated MWF solutions. The obtained information can further be used to calibrate electronic nose sensors for high-throughput and rapid analysis in future projects. Hence, it can be concluded that headspace analysis of volatile microbial metabolites by HSSE in combination with TDS-GC-MS is a suitable monitoring technique for the ageing of metalworking fluids.

In-situ sampling method (HSSE-TDS-GC-MS) during MVOC (microbial volatile organic compounds) measurements of metalworking fluids (MWF)