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17 Introduction 17 Methods 20 Sediment Collection and Handling 20 Selection of Samples for Cycle 1a and Cycle 1b Toxicity and Bioaccumulation Testing 21 Grain Size and Total Organic Carbon Analyses of Whole Sediment 22 Chemical Characterization of Whole Sediment 23 Organic Analyses 23 Inorganic Analyses 23 Chemical Characterization of Pore Water 24 Sampling of Pore Water by Centrifugation 24 Sampling of Pore Water with Peepers 24 Solid-Phase Microextraction 25 Results and Discussion 25 Physical Characterization of Whole Sediment 25 Chemical Characterization of Whole Sediment 25 Organics 25 Total Metals 26 Acid Volatile Sulfide and Simultaneously Extracted Metals 26 Chemical Characterization of Pore Water: General Water Quality, Inorganics and Dissolved Organic Carbon 27 References Cited 28

scientific investigations report

Evaluation of toxicity to the amphipod, &lt;i&gt;Hyalella azteca&lt;/i&gt;, and to the midge, &lt;i&gt;Chironomus dilutus&lt;/i&gt;; and bioaccumulation by the oligochaete, &lt;i&gt;Lumbriculus variegatus&lt;/i&gt;, with exposure to PCB-contaminated sediments from Anniston, Alabama