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v INTRODUCTION 1 Literature Review 2 RMgX 2 RMgX» solvent 3 R2% 13 Purpose 16 Computer Programs 18 STRUCTURE OF ^Br^O^(C^R^O) 21 Literature Review 21 Preparation 26 Properties and Analyses 30 Properties 30 Chemical analysis 33 Thermogravimetric analysis 36 Infrared analysis 39 Comparison with MgBrg'diethylether 54 Summery of the analytical results 55 Space Group Determination 56 Collection and Correction of Intensity Data 58 Lorentz polarization 58 Absorption 60 Collection of data on the G.E. XRD5 diffractrometer 64

Molecular configurations of some of the solvated compounds of the Grignard system