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v Chapter 1. General Introduction 1 Historical Perspectives 1 Fundamental Aspects of ICP-MS 2 ICP-MS Instrumentation 3 Blank Purity in ICP-MS 4 Previous EMLC Experiments 6 Matrix Effects in ICP-MS 7 Flow Injection in ICP-MS 9 Shielded Torch in ICP-MS 10 Dissertation Objectives and Organization 11 Figures 12 References 27 Chapter 2. Electrochemically-Modulated Liquid Chromatography for Cleaning the Blank in Inductively Coupled Plasma – Mass Spectrometry 31 Abstract 3

Developments in ICP-MS: electrochemically modulated liquid chromatography for the clean-up of ICP-MS blanks and reduction of matrix effects by flow injection ICP-MS