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The new phase, BaZnioAb, was synthesized during reactions used to explore the Ba-ZnA1 system. (a=12.267(2) A, cubic, space group FmJc (No. 226), Z = 8). BaZnioAl: is a derivative of the NaZn^ structure type containing empty icosahedral units of [ZnioAh]. Magnetic susceptibility measurements of the title compound show diamagnetic behavior. Experimental and theoretical studies indicate that the formation of filled or unfilled clusters in the NaZn^-type structure is affected by the size of the cluster, vec of the AM12+X (A = alkaline earth element, M = late transition metal and Al; 0 < x < 1), and the transition metal in the center of an icosahedral unit.

Experimental and theoretical investigations in alkaline earth-zinc-aluminum intermetallic systems