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Two x-ray methods, the single-crystal x-ray diffraction and the extended x-ray absorption fine-structure method, are studied in this thesis. The former method has long been a unique tool for the determination of crystal structures, while the latter method just became a powerful tool to determine the arrangement of atoms in any form of condensed matter in the last decade. 44 refs.

A hybrid Patterson-superposition/direct-method approach to the X-ray phase problem, and in-lab EXAFS techniques