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v CHAPTER 1. GENERAL INTRODUCTION OF FUNCTIONALIZATION OF MESOPOROUS SILICATE 1 Dissertation Organization 1 Literature Review of Functionalization of Mesoporous Silicates 3 Introduction 3 Discovery and Synthesis of Mesoporous Materials 4 Functionalization of Mesoporous Silicates 7 Applications of Functionalized Mesoporous Silicates in Catalysis 11 References 12 CHAPTER 2. ONE-POT REACTION CASCADES CATALYZED BY BASEAND ACIDFUNCTIONALIZED MESOPOROUS SILICA NANOPARTICLES 20 Abstract 20 Introduction 20 Results and Discussions 22 Conclusions 25 Acknowledgement 25 References 25 Supporting Information 31 CHAPTER 3. BIFUNCTIONALIZED MESOPOROUS MATERIALS WITH SITESEPARATED BR∅NSTED ACID AND BASE AS SUCCESSFUL COHABITATING CATALYSTS 37 Abstract 37 Introduction 37 Results and Discussions 39 Conclusions 41 Acknowledgement 42 References 42 Supporting Information 50 CHAPTER 4. MN-MODIFIED AND WELL-DEFINED RH NANOPARTICLES SUPPORTED ON MESOPOROUS SILICA NANOPARTICLES: HIGHLYSELECTIVE SYNTHESIS OF ETHANOL FROM SYNGAS 62 Abstract 62 Introduction 62 Results and Discussions 64 Conclusions 70 Acknowledgement 70 References 70 Supporting Information 80

Functionalization of mesoporous silica nanoparticles and their applications in organo-, metallic and organometallic catalysis