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Basing on temperature dependences of the light intensity transmitted through polarisation system and the birefringence of K0.2Rb1.8Cd2(SO4)3 crystals, we have determined the phase transition temperature for this solid solution. A conclusion is drawn that the monoclinic and triclinic phases on the (x, T)-phase diagram for the mixed crystals K2xRb2(1–x)Cd2(SO4)3 should disappear at the triple points occurring at x < 0.1.

Phase transitions in as-grown K0.2Rb1.8Cd2(SO4)3 langbeinite crystals: a birefringence study