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We have performed in-situ x-ray diffraction (XRD) measurements in order to acquire the information about synthesis conditions of several rare-earth transition-metal pnictides. By considering the results for a battery of the in-situ XRD measurements, we have obtained conditions optimal for synthesizing layered rare-earth zinc phosphides RZn P (R = Y and Dy) and a new filled skutterudite compound 3 3

In-situ X-ray Observation of Synthesizing Process for Rare-earth Transition-metal Pnictides under High Temperature and High Pressure