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Controllable ZnSe and ZnO structures with different morphologies were synthesized by a simple hydrothermal method. The effects of hydrazine hydrate and sodium hydroxide on the final product and morphology were studied. The results showed that controlled phase transition from ZnSe to ZnO was achieved by adjusting the volume of hydrazine hydrate. The structure variety of as-synthesized product depended on the hydrazine hydrate volume and sodium hydroxide concentration, which was further confirmed by SEM and XRD. It showed that hydrazine hydrate acted a pivotal part in the restoring process of selenium. Pure ZnSe microspheres were obtained when the volume of N H ·H O increased to 10 mL. 2 4 2

Tunable Formation of ZnSe to ZnO due to a Controlled Phase Transition Driven by Hydrazine and Sodium Hydroxide