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Cyano-bearing conjugated polycarbazoles PHN-1 and PHN-2 were efficiently prepared in high yields from corresponding monomers with paraand meta-configuration by oxidative coupling polymerization at room temperature, respectively. PHN-1 with para-configuration exhibits higher porosity than meta-configuration counterpart PHN-2. Cyano groups in the polymers were further converted to conjugated polycarbazoles containing tetrazole (PHN-1-TZ and PHN-2-TZ) or amidoxime groups (PHN-1-AO and PHN-2-AO) after treatment with NaN /NH Cl and 3 4 3

Remarkably Enhanced CO2 Uptake and Uranium Extraction by Functionalization of Cyano-bearing Conjugated Porous Polycarbazoles