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Reaction of the nitronyl nitroxide radical NIT-CH3 with Gd(hfac)3 affords a onedimensional lanthanide–nitronyl nitroxide compound: [Gd (hfac)3 (NIT-CH3)]n (1) Single crystal Xray crystallographic analysis reveals that this compound is one-dimensional chain built up by Gd(hfac)3 units bridged by radicals through their NO groups. DC magnetic susceptibilities indicate that Gd complex paramagnetic above 2.0 K.

A Gadolinium(III) complex based on Nitronyl nitroxide ligand exhibiting magnetic relaxation process