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Mesostructured γ-Al2O3 has been successfully synthesized via an ionic liquid-assisted solvent evaporation process. The results show that ionic liquid [Omim]Cl plays an important role in the formation of the mesostructure due to its strong interactions with reaction particles.The synthesized porous γ-Al2O3 has a larger specific surface area of ca. 356 m/g with wormlike pore structure. The products are characterized by N2 porosimetry, X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FT-IR), and Transmission Electron Microscopy (TEM). Keywords-alumina; ionic liquid ; mesostructure; evaporation.

Ionic Liquid Assisted Fabrication of Mesostructured -Al2O3