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Cuprous oxide (Cu2O)nanomaterial has been successfully obtained by a simple sol-gel technique. The characterization indicated that the powders have a good crystalline structure, and the synthesis was successfully controlled in nanoscale.Cyclic voltammetry (CV) revealed that Cu2O cubebox exhibited a direct electrocatalytic activity for the reduction of hydrogen peroxide (H2O2) in sodium hydroxide solution. The enzyme-less amperometric sensor used in the detection of H2O2with detection limit of 81.69μM (S/N = 3) over wide linear detection ranges up to 0.39 mM and with a high sensitivity of 444.7μA·mM −1 ·cm −2 , and a possible mechanism was also given in the paper.

Cuprous Oxide Cubebox for Nonenzymatic Amperometric Hydrogen Peroxide Detection