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Nitrogen-doped nano-sized titania(N-TiO 2)photocatalysts were prepared by sol-gel process followed by ultrasonication.The photocatalytic decomposition of methyl orange in aqueous solution was used as a probe reaction to estimate their photocatalytic activities.Applying means of XRD,TEM and UV-Vis DRS and XPS,we analyzed the crystallite sizes,the cystal pattern,the optical property of TiO2 samples. The synthesized N-TiO 2 nanocrystals are catalytically active and absorb well into the visible region up to 600 nm.N-TiO 2 showed high degradation of methyl orange under ultraviolet as well as visible light irradiation since it has small grain,wide dispersion and strong visible-light absorption.

Photocatalytic Degradation of Methyl Orange over Nitrogen-doped TiO2 Prepared by Ultrasonic Method