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cis-perhydropyrrolo[3,4-c]pyridine-3,4-dione, a kind of nontoxic and nootropic agent, was synthesized in laboratory with a milder method than literature methods. The colorless crystal was derived from ethanol solution by solvent evaporation and the crystal structure was determined by using X-ray diffraction method. The Crystal system is monoclinic and the formula is C7H10N2O2 which is different from that in the consulted reports in reference. Keywords-cis-perhydropyrrolo[3,4-c]pyridine-3,4-dione; synthesis; crystal; X-ray diffraction

Synthesis of cis-perhydropyrrolo[3,4-c]pyridine-3,4-dione and Its X-ray Structure