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Straightforward radiosynthesis protocols for 18 F-labeled radiopharmaceuticals are an indispensable but often overlooked prerequisite to successfully perform molecular imaging studies in vivo by PET. In recent years, thanks to the expansion of the 18 F chemical toolbox, structurally diverse and novel clinically relevant radiopharmaceuticals have been synthesized with both high efficiency and ready implementation. This article provides an overview of recent 18 F-labeling methodologies, specifically for B- 18 F, Si- 18 F, Al- 18 F, and iodine (III)-mediated radiofluorination via the spirocyclic iodonium ylide technology.

the journal of nuclear medicine

Recent Advances in 18F Radiochemistry: A Focus on B-18F, Si-18F, Al-18F, and C-18F Radiofluorination via Spirocyclic Iodonium Ylides