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Путем расслоения терморасширенного графита в этиловом и трет-бутиловом спиртах под действием ультразвука получены дисперсии малослойных графеновых наночастиц. Исходный терморасширенный графит получен термической обработкой в ударном режиме нагрева тройного соединения соинтеркалирования нитрата графита с уксусной и муравьиной кислотами. Проведено исследование структурных характеристик соинтеркалата нитрата графита и терморасширенного графита методом рентгенофазового анализа. Микроструктура и морфология полученных графеновых частиц исследованы методом просвечивающей электронной микроскопии. Dispersions of graphene nanoparticles were obtained by liquid phase exfoliation of thermally expanded graphite in ethanol as well as tert-butanol via sonication. Initial thermally expanded graphite was obtained by heat treatment in the shock mode of ternary graphite nitrate intercalation compound with formic and acetic acids. Investigation of the graphite nitrate intercalation compound and thermally expanded graphite structural characteristics by X-ray diffraction analysis has been carried out. The microstructure and morphology of the obtained graphene particles were studied by transmission electron microscopy.

FEW-LAYER GRAPHENE PARTICLES BASED ON THERMALLY EXPANDED COINTERCALATE OF GRAPHITE NITRATE WITH ACETIC AND FORMIC ACIDS