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LiMnxFe(1-x)PO4 olivine cathode material (x= 0.1; 0.2; 0.3 and 0.8) fabricated according to hydrothermal route. Micro-Raman spectroscopy, SEM scanning electron microscopy, UV-Vis absorption spectra and reflectance spectra methods were performed to study the characteristics of materials. The results showed that LiMnxFe(1-x)PO4 prepared materials were nano-meter in size (60100 nm) and distorted sphere-like shape. The material has bands in the Raman spectrum corresponding to the position of the bands of the pure LiFePO4 and shift slightly. The band position at 410 cm (corresponding to the position of the 2 band of the pure LiFePO4 sample) was attenuated of the sample in which Mn ion content replaced Fe ion content to 0.8 molar ratio. But the band position at 1020 cm appeared with Strengthening intensity (corresponding to the position of the 3 band of the pure LiMnPO4 sample). The optical band gap energy of samples determined according to the Tauc equation in the range of 3.33-3.5 eV.

Analysis Of Micro-Raman Spectroscopy and Optical Band Gap Energy Of LiMnxFe1-xPO4 Cathode Materials Prepared According To Hydrothermal Route