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The curing behavior of the type II photoinitiator package based on different weight ratios of oCl-HABI (hydrogen acceptor)/NPG (hydrogen donor) systems (where o-Cl-HABI is a 2chlorohexaaryl biimidazole, NPG is an N-phenylglycine) was investigated through FT-IR, gel-fraction, electron spin resonance (ESR) and photoluminescence (PL) methodologies. As the amount of NPG increasing, the faster curing speed occurred. However, the curvature photo-reactivity phenomenon was observed as the amount of o-Cl-HABI at 0.5, 1 and 2 wt%, respectively. In addition, the radical transfer mechanism in the presence of air and nitrogen atmospheres was also discussed in this study.

journal of photopolymer science and technology

Photocuring Kinetic Studies of TMPTMA Monomer by Type II Photoinitiators of Different Weight Ratios of 2-Chlorohexaaryl Biimidazole (o-Cl-HABI) and &lt;i&gt;N&lt;/i&gt;-Phenylglycine (NPG)