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A concise, rapid and high-yielding flow synthesis of aryl diazonium tetrafluoroborate salts is reported. The flow approach has been achieved by means of a diazotization reaction to access unstable aryl diazonium chloride salts in situ, followed by reaction with sodium tetrafluoroborate, to afford the corresponding aryldiazonium tetrafluoroborates in isolated yields of 64-100%.

A concise, rapid and high yielding flow synthesis of aryldiazonium tetrafluoroborates