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Photoreduction of carbon dioxide with hydrogen using temperature programmed method The photocatalytic reduction of carbon dioxide with hydrogen was studied by Temperature-Programmed Surface Reaction (TPSR). This process was carried out in a flow reactor that was especially designed and constructed for this purpose. Titanium dioxide (TiO 2 , Degussa P-25) was used as supports for platinum, ruthenium and nickel catalysts. The experimental results indicated that the activity of photoreduction of CO 2  changes as follows: Ru/TiO 2  &gt; Ni/TiO 2  &gt; = Pt/TiO 2  &gt; TiO 2 .