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Luminescence dating is widely applied nowadays, mainly for archaeological material and artefacts and sediments of all types and origins. However, optically stimulated luminescence (OSL) from archaeological sediment, originated from mud brick buildings has been hardly studied. The ar- chaeological sites of Tall Abu Fahd and Tall Qsubi are located in the Middle Euphrates Valley, Deir ez-Zor district, Syria. These two Bronze Age sites were recently discovered by a Spanish-Syrian team from the Directorate General of Antiquities and Museums (Damascus) and the University of Coruña. Both sites were dated (about 3.5 ka BC) by typological pottery classification. Sediment and pottery samples from these archaeological sites were collected for luminescence dating. Several analytical procedures for obtaining equivalent doses were tested on the sediment samples. Blue OSL from quartz subsamples and IRSL, post IRSL Blue OSL from feldspar contaminated quartz and polymin- eral subsamples were performed to obtain OSL ages. For the pottery samples, additive dose TL on a coarse grain feldspar contaminated quartz subsample was performed as well. Results have shown agreement among all the luminescence procedures tested on the Tall Abu Fahd site samples after fad- ing correction, showing ages around 2.7 ka BP. Obtained ages from the other site samples show dis- agreement among quartz blue OSL and the other subsamples. Fading ratios allow correcting age un- derestimations from the polymineral post-IR OSL signal. However, the polymineral IRSL signal still shows underestimation. Final sediment and pottery ages have shown good agreement. Older 14C inde- pendent age (3.32 ka BP) corresponds to occupational periods of the site while sediment ages are at- tributed to a post occupation phase.

TL and OSL Dating of Sediment and Pottery from Two Syrian Archaeological Sites