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The aim of the research work was to investigate the effect of superficial gas velocity and solids concentration on the critical agitator speed, gas hold-up and averaged residence time of gas bubbles in an agitated gas-solid-liquid system. Experimental studies were conducted in a vessel of the inner diameter of 0.634 m. Different high-speed impellers: Rushton and Smith turbines, A 315 and HE 3 impellers, were used for agitation. The measurements were conducted in systems with different physical parameters of the continuous phase. Liquid phases were: distilled water (coalescing system) or aqueous solutions of NaCl (non-coalescing systems). The experiments were carried out at five different values of solids concentration and gas flow rate. Experimental analysis of the conditions of gas bubbles dispersion and particles suspension in the vessel with a flat bottom and four standard baffles showed that both gas and solid phases strongly affected the critical agitation speed necessary to produce a three-phase system. On the basis of experimental studies, the critical agitator speed for all agitators working in the gas-solid-liquid systems was found. An increase of superficial gas velocity caused a significant increase of the gas hold-up in both coalescing and non-coalescing three-phase systems. The type of the impeller strongly affected the parameters considered in this work. Low values of the critical impeller speed together with the relatively short average gas bubbles residence time tR in three phase systems were characteristic for the A 315 impeller. Radial flow Rushton and Smith turbines are high-energy consuming impellers but they enable to maintain longer gas bubbles residence time and to obtain higher values of the gas hold-up in the three-phase systems. Empirical correlations were proposed for the critical agitator speed, mean specific energy dissipated and the gas hold-up prediction. Its parameters were fitted using experimental data.

Solid suspension and gas dispersion in gas-solid-liquid agitated systems