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An α, α ′ -dipyridyl adduct of a complex compound hexaaquatribenzene-1,2,4,5-tetracarbonatotetra iron (III) with porous structure was synthesized for the first time. According to the results of elemental, X-ray, IR-spectroscopic and differential-thermal analyses the individuality, chemical formula, thermal destruction, and form of coordination of acidic anion and dipyridyl were established. During interaction of a complex compound with dipyridyl, it completely loses all crystallization molecule of water resulting in a compound with a chemical formula of Fe 4 (C 6 H 2 (COO) 4 ) 3 (dpy) 2 (dipyridyl). Using the identification of diffraction pattern the parameters of lattice cell of the complex compound were determined.

journal of polymer science and engineering

Synthesis and structural-chemical studies of adduct of coordination supramolecular porous polymer hexaaquatribenzene-1,2,4,5- tetracarbonato-tetrairon(iii) with dipyridyl