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Titanium is reputed as “space metal”, characterized by its stable chemical properties, good resistance to high temperature, low temperature, strong acid and alkali, as well as the highest strength-to-density ratio of any metallic elements.1–4) In a non-alloy state, titanium is as strong as some steels, but 45% lighter. Titanium can be alloyed with aluminium, vanadium and other elements to produce strong lightweight alloys for aerospace, automobile, industrial process, agri-food and other applications.4–6) Vanadium, as one of the most important alloying elements, is widely used in metallurgy, chemical engineering and aerospace for its ability to enhance mechanical properties, such as tensile strength, hardness and fatigue resistance.7,8) With the development of economy in the 21st century, the requirements of titanium and vanadium are rapidly increasing. Furthermore, it is well known that vanadium-titanium magnetite resource is a typical multiple-element symbiotic composite ore, which contains 59.2–62.3 wt% TFe, 5.2–12 wt% TiO2, 0.8–1.02 wt% V2O5. Meanwhile, the vanadium-titanium magnetite is the largest titanium and vanadium resource in China and other countries.8,11) NeverSeparation of Vanadium and Titanium Phase from the Vanadium Slag System Utilizing Supergravity