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A combination of X-Ray Magnetic Circular Dichroism and PhotoEmission Electron Microscopy (XMCD-PEEM) was applied to the magnetic domain analysis of Nd-Fe-B sintered magnets. The XMCD-PEEM high-resolution images revealed both the magnetic domain structures and the microstructural morphologies. In the thermally demagnetized state, each grain in a polycrystalline sample exhibits a multidomain structure, which is magnetically coupled across grain boundaries. After the DC field-demagnetization, it changed to a single domain structure. The magnetization vector in each surface grain reversed to the negative direction during the field-demagnetization procedure because of the small coercivity in the surface region. In the present study, we observed this surface domain reversal for the first time by means of XMCDPEEM imaging method, which is important in order to understand the surface phenomena of Nd-Fe-B magnets. [doi:10.2320/matertrans.MRA2008141]

Magnetic-Domain Structure Analysis of Nd-Fe-B Sintered Magnets Using XMCD-PEEM Technique