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Three-dimensional (3D) configurations of 14H long-period stacking ordered (LPSO) structures formed in Mg97Zn1Gd2 cast alloys at intermediate stages of the formation process have been studied by single tilt-axis electron tomography using high-angle annular dark-field scanning transmission electron microscopy. Lateral morphology of the 14H LPSO is clearly visualized by reconstructing 3D volumes. An existence of “dent-shaped” area was found in a 3D reconstructed volume for the first time. The edge of LPSO shows a characteristic triangular shape with an angle of 60°, which indicates that the growth front is parallel to f11 20gMg. It is suggested that in-plane irregular or characteristic shapes are related to the lateral growth mechanism of LPSO. Electron tomography has proven to be an indispensable tool to characterize in-plane structural information of LPSO formed in ¡-Mg matrix. [doi:10.2320/matertrans.MH201406]

materials transactions

Three-Dimensional Shapes and Distributions of Long-Period Stacking Ordered Structures in Mg&lt;sub&gt;97&lt;/sub&gt;Zn&lt;sub&gt;1&lt;/sub&gt;Gd&lt;sub&gt;2&lt;/sub&gt; Cast Alloys Characterized by Electron Tomography