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As-quenched microstructure of the Fe-23 at% Al-7 at% Ti alloy was a mixture of (A2+D0 3 ) phases. When the as-quenched alloy was aged at 1073 K for moderate times, D0 3 domains grew preferentially along (100) directions and extremely fine B2 particles occurred at a/2(100) antiphase boundaries (APBs). After prolonged aging at 1073 K, the B2 particles would grow to occupy the whole a/2(100) APBs. Consequently, the stable microstructure of the alloy at 1073 K was a mixture of (B2+D0 3 ) phases.

Formation of (B2+D0<SUB>3</SUB>) Two-Phase Microstructure in a Fe-23 Al-7 Ti Alloy