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ZnO crystals with octahedral morphology were synthesized in large quantity using a simple thermal evaporation of ZnF2 powder in air. No catalysts and impurities were not used in the synthetic process. Scanning electron microscopy image showed that the synthesized ZnO crystals were of well-defined octahedral shape with smooth surfaces. X-ray diffraction data revealed that the octahedral-shaped ZnO crystals had a hexagonal wurtzite structure. As the synthetic temperature increased, the crystal size increased without altering the octahedral morphology. Energy dispersive X-ray spectroscopy spectrum confirmed the high purity of the ZnO crystals. Two emission peaks at around 430 and 460 nm was observed in the cathodoluminescence spectrum of the octahedral-shaped ZnO crystals. [doi:10.2320/matertrans.M2013402]

Synthesis of ZnO Crystals with Octahedral Morphology through Thermal Evaporation Technique in Air