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Low temperature synthesis of lithium­nitride compound was conducted on the lithium target for BNCT by N2/H2O mixing gas squirt in the ultra high vacuum chamber, and the following results were derived. (1) Lithium­nitride compound was synthesized on the lithium target under 101.3 Pa N2 gas squirt at room temperature and in the ultra high vacuum chamber under the pressure of 1 © 1018 Pa. (2) Remarkable contamination by O and C was observed on the lithium­nitride compound synthesized under the squirt pressure of 13.3­80 Pa/1.33­4.7 Pa N2/ H2O mixing gas. (3) No contamination and synthesis of Li­N compound was observed under the squirt pressure of 0.013­0.027Pa/0­0.005Pa N2/H2O mixing gas. (4) Contamination by O and C was enhanced with excessive addition of H2O at the pressure of over 1.33 Pa. [doi:10.2320/matertrans.M2013242]

Low Temperature and Pressure Synthesis of Lithium&ndash;Nitride Compound with H<sub>2</sub>O Addition on Lithium Target for BNCT

Low Temperature and Pressure Synthesis of Lithium–Nitride Compound with H<sub>2</sub>O Addition on Lithium Target for BNCT