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The structure of a Ni-substituted Al13(Ru,Ni)4 phase was analyzed by single crystal X-ray diffraction. The present analysis revealed the distribution of Ni at five heavy metal sites of Ru/Ni(1), Ru/Ni(2), Ru/Ni(3), Ru/Ni(4) and Ru/Ni(5). The anisotropic contraction of the corresponding coordination polyhedra around heavy metal sites was also suggested together with a variation of lattice constants as a function of Ni content. © 2011 The Japan Institute of Metals.

The Structure of an Al-Ni-Ru Monoclinic Phase Al<SUB>13</SUB>(Ru,Ni)<SUB>4</SUB>