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A unique entangled duplex structure was formed in rapidly solidified Cu­Fe­Zr­B alloys with Cu/Fe ratio = 1/1 and 6/1. Polycrystalline globules, embedded in a Cu crystalline matrix, were also observed in Cu35Fe35Zr10B20 and Cu60Fe10Zr10B20 alloys; this rapidly solidified structure was drastically different from that of Cu­Fe­Zr­B alloys enriched in Fe. Multi-step liquid phase separation can lead to unique microstructure formation during rapid solidification. [doi:10.2320/matertrans.F-M2013837]

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Entangled Duplex Structure and Polycrystalline Globule Formation through Multistep Liquid-Phase Separation in Cu&amp;ndash;Fe&amp;ndash;Zr&amp;ndash;B Alloys