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Defocus mode of Lorentz microscopy has revealed change in the magnetic microstructure with a first-order magnetic phase transition in La(Fe x Si 1 - x ) I 3 compounds (0.86 ≤ x ≤ 0.90). Upon heating specimens from the ferromagnetic phase to the paramagnetic phase, magnetic domains disappear instantaneously at the Curie temperature, concurrent with a substantial change in the volume. The observations are consistent with the feature of the first-order phase transition, which gives rise to extraordinary phenomena of these compounds such as large magnetocaloric effects.

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&lt;I&gt;In Situ&lt;/I&gt; TEM Observation of Thermally-Induced First-Order Magnetic Transition in Itinerant-Electron Metamagnetic La(Fe&lt;I&gt;&lt;SUB&gt;x&lt;/SUB&gt;&lt;/I&gt;Si&lt;SUB&gt;1&amp;minus;&lt;I&gt;x&lt;/I&gt;&lt;/SUB&gt;)&lt;SUB&gt;13&lt;/SUB&gt; Compounds