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A series of di and triorganotin(IV) complexes of the general formula,   R2(Cl)SnL (R= Me: 1; Bu: 2) and R3SnL (R = Bu: 3; Ph: 4) have been   synthesized by refluxing equivalent molar ratios of orgnotin(IV) chlorides   (R2SnCl2/R3SnCl) with the 1H-1,2,4-Triazole-3-thiol (LH) in dry methanol. The   synthesized complexes (1-4) were further treated with CS2 and R2SnCl2/R3SnCl   in 1:1:1 molar ratio to yield the homobimetallic complexes of the types   R2(Cl)SnLCS2Sn(Cl)R2 (R = Me: 5; Bu: 6) and R3SnLCS2SnR3 (R = Bu: 7; Ph: 8).   The ligand and the complexes have been characterized by elemental   microanalysis (CHNS), FT-IR and multinuclear NMR (1H&13C), and electron   ionization mass spectrometry. IR data demonstrates that the dithiocarbamate   donor site of the ligand acts in a bidentate manner and there isa trigonal   bipyramidal geometry around Sn(IV) in solid state. 1H and 13C NMR data   supports the tetrahedralgeometry with thiol donor sites of the ligand while   tetra and penta coordinated environments around dithiocarboxylate bound   tin(IV) in solution state. Mass spectrometric data supported well the   structures of the synthesized complexes. The homobimetallic derivatives were   found more active than mononuclear organotin(IV) compounds and free ligand   against various strains of bacteria and fungus

journal of the serbian chemical society

Synthesis and spectroscopic characterization of mononuclear/binuclear organotin(IV) complexes with 1H-1,2,4-triazole-3-thiol: Comparative studies of their antibacterial/antifungal potencies