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The properties of electrodeposited PbO2 are sensibly influenced by deposition   current and temperature. In particular, tritium radiotracer measurements have   demonstrated that protons are incorporated in the bulk of the oxide film and   on its surface. The degree of hydration increases with increasing current and   decreases with temperature, and is related to the morphological   characteristics of the oxide such as roughness measured by changes of the   double layer capacity. Conversely, the amount of hydrogen has negligible   effects on the number of free carriers evaluated from Mott-Schottky plots.   The hydration degree of the surface seems to be an important factor   influencing electrocatalytic processes at high potentials such as O2   evolution and O3 formation. On less hydrated, more crystalline PbO2 surfaces   the first process is inhibited, and accordingly, the second is favored

An electrochemical and radiotracer investigation on lead dioxide: Influence of deposition current and temperature